IUPAC – CORE GROUP MEETING

Bangalore 17-22 September 2006

 

The hydrogen bond is an attractive interaction between a group X–H and an atom or a group of atoms Y, in the same or different molecule(s), when there is evidence of bond formation.

 

The evidence that may be used in this context should include the criteria below.  To improve the reliability of the definition of a particular interaction as a hydrogen bond, as many of the following criteria as possible should be satisfied.

 

It is understood that there will be borderline cases for which the interpretation of the evidence might be subjective.  In any case, the exceptions to these conditions should not be gross violations, for an interaction which is termed a hydrogen bond.

 

The following criteria are recommended as evidence for a hydrogen bond X–H•••Y–(Z):

 

(1)  The physical forces involved in hydrogen bonding must include electrostatic and inductive forces in addition to London dispersive forces.*1

 

(2)  The atoms X and H are covalently bonded to one another, and the bond is polarized in X–H•••Y–Z, such that the H becomes more electropositive.

 

(3)  The lengths of the X–H bond and, to a lesser extent, of the Y–Z bond deviate from the X–H and Y–Z equilibrium values.*2

 

(4)  The X–H and Y–Z bond vibrational frequencies and intensities show changes on hydrogen bond formation and new vibrational modes associated with the formation of the H…Y bond are generated.

(5)  The X–H and Y–Z NMR nuclear chemical shielding tensors (chemical shifts) undergo changes, associated with spin-spin coupling and NOE (nuclear Overhauser enhancement) transmitted through X–H•••Y–Z.

 

(6)  The stronger the hydrogen bond, the more linear the X–H•••Y angle, θ, and the shorter the H…Y distance.*3

 

(7)  The interaction energy per hydrogen bond is greater than at least a few kT ( 1 kT = 600 cal mol–1 = 2.4 kJ mol–1 at 300 K) in order to ensure its stability.*4

 

The following characteristics are typical of hydrogen bonds:

 

(1)  The pKs of  X–H and Y–Z and the strength of any hydrogen bond formed are correlated.

 

(2)  A hydrogen bond may be involved in a proton transfer reaction.

 

(3)  Networks of hydrogen bonds show the phenomenon of cooperativity, manifest by more than additive changes in the hydrogen bond properties with an increase in network size.*5

 

(4)  Hydrogen bonds affect crystal packing and other supramolecular properties.*6

 

(5)  Theoretical estimates of charge transfer in hydrogen bonding shows that the interaction energy is highly correlated with the amount of electronic charge transferred.

 

* A more-detailed explanation to be added.